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用納升微徑色譜柱可以非常方便的提高物質(zhì)分離的靈敏度和檢測(cè)限, 可以提高5000個(gè)基數(shù)點(diǎn)比普通的4.6內(nèi)徑的柱子.

詳細(xì)介紹

德國邁克Dr.Maisch色譜柱分類包括：

圖34
圖34：Nanocolumns，納米微徑柱，微徑色譜柱

納米微徑管液相色譜柱
	用納升微徑色譜柱可以非常方便的提高物質(zhì)分離的靈敏度和檢測(cè)限, 可以提高5000個(gè)基數(shù)點(diǎn)比普通的4.6內(nèi)徑的柱子.
	1.) 規(guī)格: 150 mm x 75 µm 類型: Reprosil-Pur C18-AQ, 3 µm 貨號(hào).: R13.aq.s150.075 批次.: 120305 86401 流動(dòng)相: 乙腈 /水 (70 /30) 流速: 200 nl / min. 柱壓: 90 bars 檢測(cè)波長: UV 254 nm 結(jié)果分析: Peak 1: Nitrobenzene , RT 2.96 min. N/m = 70 000 Peak 2: Biphenyl, RT 6.8 min.N/m = 120 000


	2.) 規(guī)格: 200 mm x 75 µm 類型: Reprosil-Pur 300 ODS-3, 3 µm 貨號(hào).: R33.93.s200.075 批號(hào).: 280905 16001 流動(dòng)相:乙腈 /水 (70 /30) 流速: 200 nl / min. 壓力: 100 bars 檢測(cè)器: UV 254 nm 結(jié)果分析: Peak 1: Nitrobenzene, RT 4.65 min. N/m = 54 000 Peak 2: Biphenyl, RT 7.9 min. N/m = 95 000
	如果想增加竹子的檢測(cè)靈敏度,可以把柱子的內(nèi)徑變得更小
	Column- id (mm)	Flow (µl/min)	Increase of Sensivity
	4.6	1000	1
	2.0	200	4
	1.0	40	21
	0.5	10	85
	0.3	3	235
	0.1	0.5	2100
	0.075	0.3	3760
	Fused Silica capillary columns with		50 µm, 75 µm, 100µm, 150 µm id
	Stainless steel GLT-columns with		0.3mm0.4mm 0.5mm 0.75mm id

Reprosil-Pur C18-AQ 3um

長度	40mm	125mm	150mm	200mm	250mm
內(nèi)徑0.75mm--0.050mm,其他長度可以另詢	3750元	3900元	`4200元	4400元	4600元

可以提供各種填料類型的，各種規(guī)格內(nèi)徑長度的微徑液相色譜柱，如有疑問請(qǐng)致電本公司。

圖35
圖35：U-HPLC (Maisch) 超高壓液相色譜柱

描述	碳含量		Mat. No.

	Reprospher
	Reprospher 100 C18, 1.8 µm	16%	endc.	rs118.9e.
	Reprospher 100 C18, 2 µm	16%	endc.	rs12.9e.
	Reprospher 100 C18, 2.5 µm	16%	endc.	rs125.9e.

	Reprospher 100 C18-DE, 1.8 µm	16%	double endc.*	rs118.9de.
	Reprospher 100 C18-DE, 2 µm	16%	double endc.*	rs12.9de.
	Reprospher 100 C18-DE, 2.5 µm	16%	double endc.*	rs125.9de.

	Reprospher 100 C18-Aqua, 1.8 µm	12%	pol.Gr.+ endc.	rs118.9aq.
	Reprospher 100 C18-Aqua, 2 µm	12%	pol.Gr.+ endc.	rs12.9aq.
	Reprospher 100 C18-Aqua, 2.5 µm	12%	pol.Gr.+ endc.	rs125.9aq.

	Reprospher 100 C18-NE, 1.8 µm	15%	not endc.	rs118.90.

	Reprospher 100 Phenyl, 1.8 µm	9%	double endc.*	rs118.pde.
	Reprospher 100 Phenyl, 2 µm	9%	double endc.*	rs12.pde.
	Reprospher 100 Phenyl, 2.5 µm	9%	double endc.*	rs125.pde.

	Reprospher 100 C8-Aqua, 1.8 µm	8%	pol.Gr.+ endc.	rs118.8aq.
	Reprospher 100 C8-Aqua, 2 µm	8%	pol.Gr.+ endc.	rs12.8aq.
	Reprospher 100 C8-Aqua, 2.5 µm	8%	pol.Gr.+ endc.	rs125.8aq.

	Reprospher 100 C8, 1.8 µm	10%	endc.	rs118.8e.
	Reprospher 100 C8, 2 µm	10%	endc.	rs12.8e
	Reprospher 100 C8, 2.5 µm	10%	endc.	rs125.8e

	Reprospher 100 C8-DE, 1.8 µm	10%	double endc.*	rs118.8de.
	Reprospher 100 C8-DE, 2 µm	10%	double endc.*	rs12.8de.
	Reprospher 100 C8-DE, 2.5 µm	10%	double endc.*	rs125.8de.

	Reprospher 100 CN, 1.8 µm			rs118.C0

	*Modified with 2 endcappings: the first endcapping takes place in the liquid-form and the second additional endcapping takes place in gas-form, which makes the phases much more base deactivated than conventional single step endcapping techniques. These phases are more "inert" and more pH stable than those manufactured using with conventional endcapping techniques.

	ReproSil-Saphir
	Reprosil Saphir 100 C18, 1.8 µm	20%	endc.	ra118.9e
	Reprosil Saphir 100 C18 , 2.2 µm	20%	endc.	ra122.9e


	ReproSil-Pur Basic
	Reprosil-Pur Basic 120 C18, 1.9 µm	17 % C	double bound endc.	r119.b9.
	Reprosil-Pur Basic 120 C18, 2.5 µm	17 % C	double bound endc.	r125.b9.


	ReproSil-Pur
	ReproSil-Pur 120 C18-AQ, 1.9 µm	15 % C	endc.	r119.aq
	ReproSil-Pur 120 C18-AQ, 2.4 µm	15 % C	endc.	r124.aq.


	ReproSil-Gold Turbo

圖36
圖36：ReproGel (Maisch) 糖和有機(jī)酸分析柱

規(guī)格型號(hào): 250 x 8 mm oder 300 x 8 mm iD.
適合分析糖，有機(jī)酸，氨基酸等物質(zhì)
規(guī)格型號(hào): 250 x 8 mm or 300 mm x 8 mm ，其他規(guī)格型號(hào)可以來電詢問.
型號(hào)	應(yīng)用方面	流動(dòng)相體系	編號(hào)	對(duì)應(yīng)美國藥典
ReproGel H, 9 µm	for sugars,alcohols and acids	Water or 9mM sulfiric acid	su9.h0	L-17
ReproGel Ca, 9 µm	for sugars and alcohols	Water at 80 C°	su9.ca.	L-19
ReproGel Na, 9 µm	for sugars	Water at 80 C°	su9.na.	L-58
ReproGel Pb, 9 µm	for sugars	Water at 80 C°	su9.pb.	L-34
ReproGel Ag, 9 µm	for sugars	Water at 80 C°	su9.ag.

References of ReproGel H+
References of ReproGel Ca2+
References of ReproGel Pb2+


				Organic acids: ReproGel-H, 9 µm (250 x 8 mm) Eluent: 9 mM Sulfuric Acid, Flow rate: 1 ml/min., Det.: 210 nm



				Red Wine: ReproGel-H, 9 µm (250 x 8 mm) Eluent: Water, Flow rate: 0,7 ml/min. Temperature: 25 C°, Injection: 20 µl. Acids are retained with 20 x 4.6 mm SAX-Guard-Column.


				ReproGel-Ca, 9 µm (250 x 8 mm) Eluent: H20 Flow rate: 0,5 ml/min. Temperature: 80 C°, Detection: RI, Pressure: 35 bar



				Lactose: ReproGel-Ca, 9 µm (250 x 8mm) Eluent: water, Flow rate: 0,3 ml/min Temperature: 80 C° Detection: RI



				ReproGel-Ca, 9 µm, (250 x 8 mm) Flow rate: 0,5 ml/min Teperature.: 80 C° Detection: RI Injection: 20 µl


				Sugars: ReproGel-Pb, 9 µm (250 x 8 mm,) Eluent: H20, Flow rate: 0,3 ml/min., Temperature: 80 C°, Detection: RI, Pressure: 25 bar

圖37
圖37：Reprosil Chiral 手性色譜柱
德國Dr.maisch公司的手性色譜柱種類非常豐富，并且性價(jià)比非常高，各種型號(hào)的分析和
制備柱均可提供，在歐洲國家使用非常廣泛。

描述	美國藥典對(duì)應(yīng)編號(hào)	備注
Reprosil Chiral-OM	(USP-L40)	與大賽璐公司OD系列相對(duì)應(yīng)
Reprosil Chiral AM	(USP-L51)	與大賽璐公司AD系列相對(duì)應(yīng)
Reprosil Chiral-NR&ReproSil Chiral-NRR		ReproSil Chiral-NR 與 ReproSil Chiral-NRR色譜柱之間您可以隨意的切換流動(dòng)相，使用起來非常方便。這個(gè)色譜柱非常適合有芳香物質(zhì)中O原子接近手性中心的物質(zhì)拆分。

-> Chiral NR/AM/OM <-三個(gè)色譜柱的相比較

Reprosil Chiral-AA		ReproSil手性-AA是專為未衍生氨基酸的手性分離。這一階段還顯示了對(duì)惡唑烷酮，海因，二氮雜亞砜和良好的選擇性。它是基于超純Reprosil100二氧化硅。用手性選擇劑：芳香族化合物，共價(jià)結(jié)合到一個(gè)8微米的二氧化硅微球

Reprosil Chiral-OH		該Reprosil手性-OH是專為芳香酒精化合物的手性分離。OH基團(tuán)共價(jià)結(jié)合于超純Reprosil100二氧化硅。 zui成功分離的手性化合物是： 1）芳香族化合物 2）具有OH基的手性中心。

Reprosil Chiral-PS		手性ReproSil-PS是專為手性芳族化合物，它含有P或S原子的分離

Reprosil Chiral-CA		ReproSil手性-CA是專為手性芳香羧酸的分離。

Reprosil Chiral-AMS		與大賽璐AS-H色譜柱相對(duì)應(yīng)

Reprosil Chiral-CM		與大賽璐OC-H色譜柱相對(duì)應(yīng)

Reprosil Chiral-JM		與大賽璐OJ-H色譜柱相對(duì)應(yīng)

Reprosil Chiral-ZM		與大賽璐OZ-H色譜柱相對(duì)應(yīng)

Reprosil Chiral-ZA		與Epitomize 1K色譜柱相對(duì)應(yīng)

Reprosil Chiral-YM		與大賽璐AY-H色譜柱相對(duì)應(yīng)

Reprosil Chiral-BM		與大賽璐OB-H色譜柱相對(duì)應(yīng)

Reprosil -AGP	(USP-L41)

Reprosil-HSA

ReproSil Chiral-TAG	USP-L63	適合分析Aminoalkohols，N-阻斷氨基酸，α-羥基酸，Oxazolidinons，海因，酰亞胺，氨基酸類

Reprosil Chiral-TG		適合分析芴甲氧羰?；?nbsp;和丹磺酰氯保護(hù)的氨基酸

Reprosil Chiral CD	USP-L45	USP-L45（丹酰-氨基酸，巴比妥類，普萘洛爾，磺胺類藥物，Prostaglandines）

Reprosil Chiral-D-PhenylGlycin	(USP-L36)	刷型 D-苯基甘氨酸，適合分析布比卡因

Reprosil Chiral-l-Prolin	(USP-L32)	Reprosil手性-L-脯氨酸，5微米° 對(duì)于DL-Atrolactinacid，DL-扁桃酸，DL-乳酸，DL-天冬酰胺; DL-塞林，DL-苯丙氨酸，DL-蘇氨酸，DL-脯氨酸，DL-組氨酸，625， - DL-華菱，DL-酪氨酸，DL-色氨酸可以很好的分析。

圖38
圖38：ReproSil 70/100/300 系列色譜柱
多孔球狀二氧化硅：3，5，10微米
孔徑：70 A°/500平方米/克，100 A°/280平方米/克，300 A°/100平方米/克
孔體積：0.9，1.1毫升/克
的色譜柱,非常適合做制備，穩(wěn)定的重復(fù)性和低壓的設(shè)計(jì)。

References of ReproSil 70 C18
References of ReproSil 100 C18
References of ReproSil 100 C8
References of ReproSil 100 ODS-A
References of ReproSil 100 Phenyl
References of ReproSil 300 C18

描述	碳含量	封尾	編號(hào)
ReproSil 70 Si, 5 µm			r05.06.

ReproSil 70 C18, 3 µm	20 % C	endc.	r03.96.
ReproSil 70 C18, 5 µm	20 % C	endc.	r05.96.

ReproSil 70 C8, 5 µm	14 % C	endc.	r05.86.
ReproSil 70 C4, 5 µm	10 % C	endc.	r05.46.
ReproSil 70 Phenyl, 5 µm	16 % C	endc.	r05.pe.
ReproSil 70 CN, 5 µm	10 % C	endc.	r05.c6.
ReproSil 70 Diol, 5 µm	4 % C		r05.d6.
ReproSil 70 NH2, 5 µm	5 % C		r05.a6.
with 100A° pores
ReproSil 100 Si, 3 µm			r13.06.
ReproSil 100 Si, 5 µm			r15.06.
ReproSil 100 Si, 10 µm			r10.06.

ReproSil 100 C4, 3 µm	5 % C	endc.	r13.46.
ReproSil 100 C4, 5 µm	5 % C	endc.	r15.46.
ReproSil 100 C4, 10 µm	5 % C	endc.	r10.46

ReproSil 100 C8, 3 µm	8 % C	endc.	r13.86.
ReproSil 100 C8, 5 µm	8 % C	endc.	r15.86.
ReproSil 100 C8, 10 µm	8 % C	endc.	r10.86.
ReproSil 100 C8-AB, 5 µm	8 % C	endc.	r15.8b.

ReproSil 100 C18, 3 µm	15 % C	endc.	r13.96.
ReproSil 100 C18, 5 µm	15 % C	endc.	r15.96.
ReproSil 100 C18, 7 µm	15 % C	endc.	r17.96.
ReproSil 100 C18, 10 µm	15 % C	endc.	r10.96.
ReproSil 100 C18-AB, 5 µm	16 % C	endc.	r05.9b.

ReproSil 100 ODS-A, 3µm	16 % C	endc.	r13.9a.
ReproSil 100 ODS-A, 5µm	16 % C	endc.	r13.9a.

ReproSil 100 Phenyl, 3 µm	9 % C	endc.	r13.p6.
ReproSil 100 Phenyl, 5 µm	9 % C	endc.	r15.p6.

ReproSil 100 CN, 3 µm	2 % C		r13.c6.
ReproSil 100 CN, 5 µm	2 % C		r15.c6.
ReproSil 100 CN, 10 µm	2 % C		r10.c6.

ReproSil 100 NH2, 3 µm	3 % C		r13.a6
ReproSil 100 NH2, 5 µm	3 % C		r15.a6
ReproSil 100 NH2, 10 µm	3 % C		r10.a6

ReproSil 100 Diol, 5 µm	3 % C		r15.d6.

ReproSil 100 C30-m, 5µm	(monomer) endc.		st15.3m.
ReproSil 100 CAT, 7 µm	simult.D.Mono-+Dival.Cations		r17.cat.

ReproSil DIBS-RP, 5µm	for Direct Injection of Biological Samples

ReproSil WP-300	for Proteins and Peptides
with 300A° pores
ReproSil 300 C4, 5 µm	2.5% C	endc.	r35.46.
ReproSil 300 C4, 10 µm	2.5% C	endc.	r30.46.

ReproSil 300 C8, 5 µm	4 % C	endc.	r35.86.
ReproSil 300 C8, 10 µm	4 % C	endc.	r30.86.

ReproSil 300 C18, 5 µm	9 % C	endc.	r25.96.
ReproSil 300 C18, 5 µm	7 % C	endc.	r35.96.
ReproSil 300 C18, 10 µm	7 % C	endc.

圖39
圖39：ReproSil-Pur系列色譜柱
多孔球形二氧化硅：1.9微米，2.5微米，3微米，5微米，7微米，10微米
孔徑/面積：60A°/500平方米/克; 120A°/300平方米/克 200A°/200平方米/克; 300A°/100平方米/克
硅膠純度>99.999％
適用于所有類型的樣品

耐酸耐堿環(huán)境下非常穩(wěn)定


	Reprosil-Pur C18-AQ			Reprosil-Pur C18-AQ			Reprosil-Pur ODS-3
120			120			120
100			100			100
80			80			80
60			60			60
40			40			40
20			20			20
	80	240 h		80	240 h		80	240 h

References of ReproSil-Pur 120 C4
References of ReproSil-Pur 300 C4
References of ReproSil-Pur 100 NH2
References of ReproSil-Pur 120 NH2
References of ReproSil-Pur C18 AQ
References of ReproSil-Pur 120 ODS-3
References of ReproSil-Pur 200 ODS-3
References of ReproSil-Pur 300 ODS-3
References of ReproSil-Pur 120 RP18-NE

描述	碳含量	封尾	編號(hào).
with 120A° pores
ReproSil-Pur 120 Si, 3 µm			r13.00.
ReproSil-Pur 120 Si, 5 µm			r15.00.
ReproSil-Pur 120 Si, 10 µm			r10.00.


ReproSil-Pur 120 C1, 3 µm	4 % C	endc.	r13.1e.
ReproSil-Pur 120 C1, 5 µm	4 % C	endc.	r15.1e.

ReproSil-Pur 120 C4, 3 µm	7 % C	endc.	r13.4e.
ReproSil-Pur 120 C4, 5 µm	7 % C	endc.	r15.4e.
ReproSil-Pur 120 C4, 10 µm	7 % C	endc.	r10.4e

ReproSil-Pur 120 C8, 3 µm	9 % C	endc.	r13.8e.
ReproSil-Pur 120 C8, 5 µm	9 % C	endc.	r15.8e.
ReproSil-Pur 120 C8, 10 µm	9 % C	endc.	r10.8e.

ReproSil-Pur 120 C18-AQ, 1.9 µm	15 % C	endc.	r119.aq.
ReproSil-Pur 120 C18-AQ, 2.4 µm	15 % C	endc.	r124.aq.
ReproSil-Pur 120 C18-AQ, 3 µm	15 % C	endc.	r13.aq.
ReproSil-Pur 120 C18-AQ, 5 µm	15 % C	endc.	r15.aq.
ReproSil-Pur 120 C18-AQ, 7 µm	15 % C	endc.	r17.aq.
ReproSil-Pur 120 C18-AQ, 10 µm	15 % C	endc.	r10.aq.

References of ReproSil-Pur C18 AQ

ReproSil-Pur 120 ODS-3, 3 µm	17 % C	endc.	r13.93.
ReproSil-Pur 120 ODS-3, 5 µm	17 % C	endc.	r15.93.
ReproSil-Pur 120 ODS-3, 10 µm	17 % C	endc.	r10.93.

ReproSil-Pur 120 RP18-NE, 3 µm	12 % C	not endcapped!	r13.90.
ReproSil-Pur 120 RP18-NE, 5 µm	12 % C	not endcapped!	r15.90.

ReproSil-Pur 120 Phenyl, 3 µm	8 % C	endc.	r13.pe
ReproSil-Pur 120 Phenyl, 5 µm	8 % C	endc.	r15.pe.
ReproSil-Pur 120 Phenyl, 10 µm	8 % C	endc.	r10.pe.

ReproSil-Pur 120 CN, 3 µm	7 % C	endc.	r13.ce.
ReproSil-Pur 120 CN, 5 µm	7 % C	endc.	r15.ce.
ReproSil-Pur 120 CN, 10 µm	7 % C	endc.	r10.ce.

ReproSil-Pur 120 NH2, 3 µm	4 % C		r13.a0.
ReproSil-Pur 120 NH2, 5 µm	4 % C		r15.a0.
ReproSil-Pur 120 NH2, 10 µm	4 % C		r10.a0.

ReproSil-Pur 120 Diol, 3 µm	7 % C		r13.d0.
ReproSil-Pur 120 Diol, 5 µm	7 % C		r15.d0.
ReproSil-Pur 120 Diol, 10 µm	7 % C		r10.d0.

200A 和 300A 孔徑適合分析多肽和蛋白
with 200A° pores
ReproSil-Pur 200 C18-AQ, 3 µm	11 % C	endc.	r23.aq.
ReproSil-Pur 200 C18-AQ, 5 µm	11 % C	endc.	r25.aq.

ReproSil-Pur 200 ODS-3, 3 µm	12 % C	endc.	r23.93.
ReproSil-Pur 200 ODS-3, 5 µm	12 % C	endc.	r25.93.

with 300A° pores
ReproSil-Pur 300 Si, 3 µm			r33.00.
ReproSil-Pur 300 Si, 5 µm			r35.00.
ReproSil-Pur 300 Si, 10 µm			r30.00.

ReproSil-Pur 300 C4, 3 µm	2,5 % C	endc.	r33.4e.
ReproSil-Pur 300 C4, 5 µm	2,5 % C	endc.	r35.4e.
ReproSil-Pur 300 C4, 10 µm	2.5 % C	endc.	r30.4e

ReproSil-Pur 300 C8, 3 µm	4 % C	endc.	r33.8e.
ReproSil-Pur 300 C8, 5 µm	4 % C	endc.	r35.8e.
ReproSil-Pur 300 C8, 10 µm	4 % C	endc.	r30.8e

ReproSil-Pur 300 ODS-3, 3 µm	9 % C	endc.	r33.93.
ReproSil-Pur 300 ODS-3, 5 µm	9 % C	endc.	r35.93.
Reprosil-Pur 300 ODS-3, 10 µm	9 % C	endc.	r30.93

ReproSil-Pur 300 Phenyl, 3 µm	3 % C	endc.	r33.pe
ReproSil-Pur 300 Phenyl, 5 µm	3 % C	endc.	r35.pe.

圖40
圖40: Reprosil-Gold (Maisch)系列
多孔球形硅膠：3微米，5微米，10微米
孔徑/面積：120A°/300平方米/克，200A°/200平方米/克，300A°/100平方米/克
超純石英。純度>99.999％
雙封尾額外的穩(wěn)定


Features of Reprosil Gold and Reprosil-Pur Basic, the High-Purity Phases (99.999%)
Phase:	Pores	S.A. (m2/g)	% Carbon	Particle sizes	Mat. No.:
Reprosil-Pur Basic C18	100 A	450	17%	1.8, 2, 3, 5, 10	r1x.b9
Reprosil-Pur Basic C18-HD	100 A	450	25%	3, 5, 10	r1x.b9h
Reprosil-Pur Basic C8	100 A	450	15%	3, 5, 10	r1x.b8
Reprosil-Pur Basic C8-2	100 A	450	12%	3, 5, 10	r1x.b82

Reprosil Gold C18	120 A	320	20%	3, 5, 10	r1x.9g
Reprosil Gold 200 C18	200 A	180	14%	5, 10	r2x.9g
Reprosil Gold 300 C18	300 A	120	8%	5, 10	r3x.9g

Reprosil Gold C8	120 A	320	12%	3, 5, 10	r1x.8g
Reprosil Gold 200 C8	200 A	180	8%	5, 10	r2x.8g
Reprosil Gold 300 C8	300 A	120	5%	5, 10	r3x.8g

Reprosil Gold C4	120 A	320	8%	3, 5, 10	r1x.4g
Reprosil Gold 200 C4	200 A	180	5%	5, 10	r2x.4g
Reprosil Gold 300 C4	300 A	120	3%	5, 10	r3x.4g


描述	碳含量	封尾方式（雙封尾）	編號(hào)
with 120A° pores
Reprosil-Gold 120 C18, 3 µm	20 % C	double bound endc.*	r13.9g
Reprosil-Gold 120 C18, 5 µm	20 % C	double bound endc.*	r15.9g
Reprosil-Gold 120 C18, 10 µm	20 % C	double bound endc.*	r10.9g

Reprosil-Gold 120 C8, 3 µm	12 % C	double bound endc.*	r13.8g
Reprosil-Gold 120 C8, 5 µm	12 % C	double bound endc.*	r15.8g
Reprosil-Gold 120 C8, 10 µm	12 % C	double bound endc.*	r10.8g
Reprosil-Gold 120 C8, 20 µm	12 % C	double bound endc.*	r120.8g
Reprosil-Gold 120 C4, 3 µm	8 % C	double bound endc.*	r13.4g
Reprosil-Gold 120 C4, 5 µm	8 % C	double bound endc.*	r15.4g
Reprosil-Gold 120 C4, 10 µm	8 % C	double bound endc.*	r10.4g
Reprosil-Gold 120 C4, 20 µm	8 % C	double bound endc.*	r120.4g

Reprosil-Gold 120 C2, 5 µm (USP-L16)	4 % C	double bound endc.*	r15.2g

with 200A° pores
Reprosil-Gold 200 C18, 3 µm	14 % C	double bound endc.*	r23.9g
Reprosil-Gold 200 C18, 5 µm	14 % C	double bound endc.*	r25.9g
Reprosil-Gold 200 C18, 10 µm	14 % C	double bound endc.*	r20.9g
Reprosil-Gold 200 C8, 5 µm	8 % C	double bound endc.*	r25.8g
Reprosil-Gold 200 C8, 10 µm	8 % C	double bound endc.*	r20.8g
Reprosil-Gold 200 C4, 5 µm	5 % C	double bound endc.*	r25.4g
Reprosil-Gold 200 C4, 10 µm	5 % C	double bound endc.*	r20.4g

with 300A° pores
Reprosil-Gold 300 C18, 3 µm	8 % C	double bound endc.*	r33.9g
Reprosil-Gold 300 C18, 5 µm	8 % C	double bound endc.*	r35.9g
Reprosil-Gold 300 C18, 10 µm	8 % C	double bound endc.*	r30.9g

Reprosil-Gold 300 C8, 3 µm	5 % C	double bound endc.*	r33.8g
Reprosil-Gold 300 C8, 5 µm	5 % C	double bound endc.*	r35.8g
Reprosil-Gold 300 C8, 10 µm	5 % C	double bound endc.*	r30.8g

Reprosil-Gold 300 C4, 3 µm	3 % C	double bound endc.*	r33.4g
Reprosil-Gold 300 C4, 5 µm	3 % C	double bound endc.*	r35.4g
Reprosil-Gold 300 C4, 10 µm	3% C	double bound endc.*	r30.4g

Reprosil-Gold 300 C2, 5 µm	1% C	double bound endc.*	r35.1g

圖41
圖41：Dr.Maisch HPLC 的選擇指南
德國邁可（DR.Maisch）公司是的專業(yè)的色譜耗材生產(chǎn)商，憑借其20多年的研發(fā)、生產(chǎn)經(jīng)驗(yàn)和*的裝填技術(shù)，打造出多個(gè)系列的高性能的色譜柱，是您分析和方法的得力工具。

Column Selection Guide:


		ReproSil-Pur 60 Si ReproSil 80 Si ReproSil 100 Si ReproSil-Pur 120 Si Equisil Si Gold-Turbo 100 Si ReproSil 80 CN ReproSil 80 NH2 ReproSil 100 CN ReproSil 100 NH2 Equisil CPS Equisil APS ReproSil-Pur CN ReproSil-Pur NH2 ReproSil 80 OH (Diol) ReproSil 100 OH (Diol) ReproSil 80, C1, C6, C8, ODS-1, ODS-2, Phenyl ReproSil 100 C4, C8, C18, Phenyl ReproSil-Pur C4, C8, Phenyl, RP18-Ne, C18-AQ, ODS-3 Equisil MOS, ODS, BDS-C8, BDS-C18 Stability C30, C30p, C30m, BS-C13, BS-C17, BS-C23, Amid-C12, Amid-C18, Amino-C8, Amino-ODS, Fluosil Fluofix 120 E, 120 N Gold-Turbo 100 ODS, 80 ODS-3, ODS-4, BS-C23, Amid-C12 Reversed phases (see obove): but with Ionization Control or Ion-Pair Agents: Ion-exchange: ReproSil 100 CAT (simult. Anions+Cations) ReproSil 80 NH2, ReproSil 100 NH2, ReproSil-Pur NH2, Equisil APS, Gold-Turbo NH2 ReproSil Polyamine Stability BS-C13, BS-C17, BS-C23 ReproSil 80 SAX, SCX ReproGel AX, AXS (Polymeric anion-phases) Reversed-Phase Mode with Wide-Pore material: ReproSil 300 C4, C8, C18 ReproSil-Pur 200 C18-AQ, ODS-3 ReproSil-Pur 300 ODS-3 Stability 300 Amid C25 Fluofix 300 E, N ReproGel NP (Non Porous) Reversed phases with Wide-Pores (see obove): but with Ionization Control or Ion-Pair Agents: Ion-Exchange with Wide-Pore material: Stability 300 Polyamine, Stability 300 BS-C23









































	ReproSil® is a tradename of Dr. Maisch GmbH. Stability®, Equisil® and Gold-Turbo® are tradenames of Dr.Maisch GmbH and / or Cil, France. Fluofix® is a tradename of Neos, Japan.

編號(hào)	填料描述	對(duì)應(yīng)型號(hào)
USP-L1	Octadecyl silane / C18, RP18, ODS) b chemically bonded to porous or ceramic silica microparticles, 1.8 untill 10 μm	Reprosil 100 C18 ( XBD) Reprosil-Pur C18-AQ Reprosil-Pur ODS-3 Reprosil Gold C18 Reprosil Saphir C18 Reprosil 80 ODS-2 Reprosil-Pur Basic C18 (HD) Reprospher C18 (DE) Equisil ODS Equisil BDS C18 Reprobond C18 Repropack C18 ReproShell C18 (Coreshell)
USP-L3	多孔硅膠微粒，即一般的硅膠柱	Reprosil 100 Si Reprosil-Pur Si Reprosil 80 Si Reprospher Si Equisil 120 Si
USP-L7	全多孔硅膠微粒鍵合C8官能團(tuán)固定相	Reprosil 100 C8 Reprosil-Pur C8 Reprosil Gold C8 Reprosil -Pur Basic C8 (HD) Reprosil 80 C8 Reprospher C8 (DE) Equisil BDS C8
USP-L8	全多孔硅膠微粒鍵合非交聯(lián)NH2固定相	Reprosil 100 NH2 Reprosil 80 NH2 Reprospher NH2 Equisil APS
USP-L9	強(qiáng)酸性陽離子交換基團(tuán)鍵合全多孔不規(guī)則形硅膠固定相，即SCX柱	Reprosil 80 SCX Reprosil Saphir SCX
USP-L10	多孔硅膠微球鍵合氰基固定相（CN），簡(jiǎn)稱CN柱	Reprosil 100 CN Reprosil-Pur CN Reprosil 80 CN Reprospher CN ( DE) Equisil CPS
USP-L11	鍵合苯基多孔硅膠微球固定相，簡(jiǎn)稱苯基柱	Reprosil 100 Phenyl Reprosil-Pur Phenyl Reprosil 80 Phenyl Reprospher Phenyl (DE) Equisil Phenyl
USP-L13	三乙基硅烷化學(xué)鍵合全多孔硅膠微球固定相（C1），簡(jiǎn)稱C1柱	Reprosil-Pur C1 Reprosil 80 C1 Equisil SAS
USP-L14	10mm硅膠化學(xué)鍵合強(qiáng)堿性季銨鹽陰離子交換固定相，簡(jiǎn)稱SAX柱	Reprosil 80 SAX
USP-L15	己基硅烷化學(xué)鍵合于*多孔性微粒硅，粒徑3-10u。	Reprosil 80 C6
USP-L16	二甲基硅烷化學(xué)鍵合于*多孔性微粒硅，粒徑3-10u。	Reprosil Gold 120 C2 Reprosil Gold 300 C2
USP-L17	由磺化的苯乙烯-二乙烯基苯交連共聚物組成的氫型陽離子交換樹脂，粒徑7-11u	Reprogel H+, 9 μm
USP-L18	氨基和氰基化學(xué)鍵合于多孔微粒硅，粒徑3-10u。	Reprosil PAC
USP-L19	由磺化的苯乙烯-二乙烯基苯交連共聚物組成的鈣型陽離子交換樹脂，粒徑7-11u	Reprogel Ca++
USP-L20	二甲氧基丙烷基化學(xué)鍵合于多孔硅膠微粒，粒徑5-10u。	Reprosil 100 Diol Reprosil-Pur Diol Reprosil 80 Diol
USP-L21	剛性球形苯乙烯-二乙烯基苯共聚物，粒徑5-10u。	Repromer 100 RPS Repromer 300 RPS Repromer 1000 RPS
USP-L22	由多孔聚苯乙烯凝膠和磺酸基組成的陽離子交換樹脂，粒徑約為10u。	Reprogel SCX
USP-L26	丁基硅烷化學(xué)鍵合全多孔硅膠微球固定相，即C4柱	Reprosil 100 C4 Reprosil-Pur C4 Reprosil Gold C4 Reprospher C4 (DE)
USP-L32	L-脯氨酸銅配合物共價(jià)鍵合于不規(guī)則形硅膠微粒的配位體的交換手性色譜填料	Reprosil Chiral-L-Hydroxy-Prolin
USP-L34	鉛型磺化交聯(lián)苯乙烯－二乙烯基苯共聚物強(qiáng)陽離子交換樹脂，9mm球形	Reprogel Pb, 9 μm
USP-L36	5mm胺丙基硅膠鍵合L-苯基氨基乙酸－3,5二硝基苯甲酰	Reprosil Chiral-PhenylGlycin
USP-L37	適合分離分子量2000～40000MW的聚甲基丙烯酸酯凝膠	Repromer OH-60, 10 μm
USP-L38	水溶性甲基丙烯酸酯基質(zhì)SEC色譜柱	Repromer OH, 10 μ
USP-L40	Tris 3,5－二甲基苯基氨基甲酸酯纖維素涂覆多孔硅膠微球	Reprosil Chiral-OM
USP-L41	球形硅膠表面固定α1酸糖蛋白固定相	Chiral-AGP
USP-L43	硅膠微球鍵合五氟代苯基固定相	Reprosil Fluosil PFP
USP-L45	β-環(huán)糊精鍵合多孔硅膠微球	Reprosil Chiral Beta-CD Reprosil Chiral Beta-PM
USP-L47	*胺鍵合高容量陰離子交換微粒	PRPX-110 RCX-10 RCX-30
USP-L51	多孔球形硅膠表面涂覆有直鏈淀粉-三(3,5-二甲苯基氨基甲酸酯)	Reprosil Chiral-AM
USP-L58	7-11um磺化交聯(lián)苯乙烯-二乙烯基苯共聚物鈉型陽離子交換樹脂	Reprogel Na+
USP-L60	小于10um的球形多孔硅膠顆粒表面共價(jià)鍵和*封端的烷基氨基化合物	Reprosil ABZ-Amid C18
USP-L62	C30硅烷鍵合全多孔硅膠	Stability C30
USP-L63	6-30um磺化交聯(lián)苯乙烯-二乙烯基苯共聚物鈉型陽離子交換樹脂	Reprosil Chiral-TAG
USP-L70	硅膠表面涂覆有纖維素-三(苯基氨基甲酸酯)	Reprosil Chiral-CM

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